Solution
Your current position:
Homepage
/
/
Dioxane Solvent Recovery

Dioxane Solvent Recovery

  • Categories:Solution
  • Author:
  • Origin:
  • Time of issue:2022-07-29
  • Views:0

(Summary description)

Dioxane Solvent Recovery

(Summary description)

  • Categories:Solution
  • Author:
  • Origin:
  • Time of issue:2022-07-29
  • Views:0
Information

Technology Introduction

Many solvents can form azeotropic and near-boiling mixtures with water, and it is difficult to further concentrate to a higher purity by using common rectification techniques. Traditional solvent dehydration processes such as rectification, azeotropic rectification, pressure swing distillation, pressure swing Adsorption, desiccant, etc. have problems such as high energy consumption, low yield, unfriendly environment, complicated operation, and low product quality.

Molecular sieve membrane dehydration technology is driven by the vapor partial pressure difference of the components, and utilizes the difference in the dissolution ( adsorption ) -diffusion rate of the components in the membrane pores and the difference in molecular size to achieve the separation between components, which is not affected by the vapor-liquid equilibrium of the separation system. It has high single-stage separation efficiency and is especially suitable for the separation of azeotropic and near-boiling mixtures. The packing density of the second-generation four-channel hollow fiber membrane is more than 3 times that of the tubular membrane , and the flux is more than 2 times. At the same time, give full play to the advantages of the membrane process in and out of the gas phase, breaking the azeotropic point, and the tower has the advantages of removing impurities and separating organic components to achieve process optimization!

 

name

Ethanol dehydration (water 10→0.5%)

Isopropyl alcohol dehydration (water 15→0.5%)

azeotropic distillation

Molecular sieve membrane

Flake alkali absorbs water

Molecular sieve membrane

Steam (t/t)

~2

~0.5

0.8

0.5

yield

~92%

>99%

~92%

>99%

third component

Have

none

Have

none

waste water

Have

none

Have

none

Operating cost (yuan/t)

~550

~200

~800

~230

 

name

Dehydration of tetrahydrofuran (water 5→0.05%)

Acetonitrile dehydration (water 25→1%)

Flake alkali absorbs water

Molecular sieve membrane

Extractive distillation

Molecular sieve membrane

Steam (t/t)

~0.75

~0.3

~2

~0.5

yield

~85%

>99%

>95%

>99%

third component

Have

none

Have

none

waste water

Have

none

Have

none

Operating cost (yuan/t)

~750

~220

~500

~200

 

Flow chart

Dioxane solvent recovery is shown in the following figure:

 

111

 

Process advantage

1 ) No third component is added, no waste liquid is discharged, and the yield is high. 2 ) Using the membrane distillation coupling technology, the process is simple and the operation energy consumption is low. 3 ) Easy to operate and high degree of automation.

 

 

Project display

Customer: On-site installation of a new material Co., Ltd. in Xuzhou    is shown in the figure below:

1

 
56 tons / day dioxane solvent recovery technical indicators :
 

project

Technical indicators

finished product

Dioxane≥99.9%
Triethylamine≤0.001%
Water≤0.01%

Exterior

Colorless and transparent

 
 

Scan the QR code to read on your phone

The research institution approved by Nanjing is also an independent legal entity of the first professional research institute of Jiangsu Industrial Technology Research Institute Membrane Science and Technology Research Institute, which is positioned as the organizer of membrane material industry cultivation.

Service hotline

E-mail:kewei@jsmst.net

Address: No. 1, Garden Train of Thought, Jiangbei New District, Nanjing

官方手机站

Mobile station

微信业务咨询

WeChat

Copyright © 2022 Nanjing Membrane Material Industry Technology Research Institute Co., Ltd  All Rights Reserved      苏ICP备2022019599号-1   seo